dc.contributor.advisor | Güneş, Bilal | |
dc.contributor.author | Dilek, Nefise | |
dc.date.accessioned | 2020-12-10T14:06:07Z | |
dc.date.available | 2020-12-10T14:06:07Z | |
dc.date.submitted | 2000 | |
dc.date.issued | 2018-08-06 | |
dc.identifier.uri | https://acikbilim.yok.gov.tr/handle/20.500.12812/304575 | |
dc.description.abstract | 2,4DIMETHOXYBENZYLÎDENE-2-HYDROXYANILINE KRİSTALİNİN X-ISINLARI KIRINIM YÖNTEMİ İLE YAPI ÇÖZÜMÜ (Yüksek Lisans Tezi) Nefise DİLEK GAZİ ÜNİVERSİTESİ FEN BİLİMLERİ ENSTİTÜSÜ Ocak 2000 ÖZET Bu çalışmada kristal verileri aşağıda' belirtilen kristalin x-ışını tek kristaf kırınım yöntemi ile yapı çözümü yapılmıştır. C,5H15N03: a = 9.732(2) Â, b = 14.299(2) Â, c = 19.083(3) Â, cc = 90.00°, P = 90.00°, y = 90.00°, Ortorombik P 2,2,2, (No: 19), M = 514.56 a.k.b., Z = 4, V = 2656.9 (8) Â3, Dx = 1.286 gr/cm3, T = 293 (2) K, XMoKa = 0.71073 Â, u( MoKa ) = 0.09 mm`1, R = 0.0615, ©R = 0.2133, GooF =1.521, (A/pU* =0.052, Apmax = 0.197 eÂ`3, Apmin = -0.203 eÂ`3. Bu çalışmada veri toplama ve Lorentz-Polarizasyon düzeltmeleri CAD-4 otomatik difraktometresi ile yapıldı. Toplanan verilere ^-scan yöntemi ile empirik soğurma düzeltmesi uygulandı. Kristal yapı SHELXS-86 programı yardımıyla direkt yöntemlerle çözüldü. Arıtım, full-matrix en küçük kareler yöntemi kullanılarak SHELXL-97 programı ile yapıldı. Kristalin molekül yapısı ORTEP-III çizim programı kullanılarak çizildi. Bilim kodu Anahtar Kelimeler Sayfa Adedi Tez Yöneticisi 404.05.01 X-ışını, Difraksiyon, Kristal yapı çözümü 104 Yrd.Doç.Dr. Bilal GÜNEŞ ^3SSS£rwMU' | |
dc.description.abstract | THE STRUCTURE DETERMIMATION OF CRYSTAL OF 2,4DIMETHOXYBENZYLIDENE-2-HYDROXYANILINE BY X-RAY DIFFRACTION METHOD (M. Sc. Thesis) Nefise DİLEK GAZI UNIVERSITY INSTITUTE OF SCIENCE AND TECHNOLOGY January 2000 ABSTRACT In this study, the structure of crystal which parameters are given as below has been determinated by x-ray diffraction method. Ci5HI5N03: a = 9.732(2) Â, b = 14.299(2) Â, c = 19.083(3) Â, a = 90.00°, (3 = 90.00°, y = 90.00°, Orthorhombic P 2ı2ı2, (No:19). M = 514.56 a.m.u., Z - 4, V = 2656.9 (8) A3, Dx = 1.286 gr/cm3, T = 293 (2) K, XMoKa = 0.71073 Â, u( MoK« ) = 0.09 mm`1, R = 0.0615, coR = 0.2133, GooF =1.521, (A/pU =0.052, Apmax = 0.197 eA'/ Apmin = -0.203 eA°. In this study data collection and Lorentz-Polarization corrections were performed by the use of CAD-4 diffractometer. An empirical absorbtion correction based on T-scan method was applied to collected data. The crystal structure was solved by direct methods by the use of SHELXS-86 software. The structure refinement was carried out by using full-matrix least-square method by the use of SHELXL-97 software. The molecular graphic of crystal was drawn by ORTEP-III plotting program. Science code Key words Page number Adviser 404.05.01 X-ray, diffraction, crystal structure determination 104 Yrd.Doç.Dr. Bilal GÜNEŞ | en_US |
dc.language | Turkish | |
dc.language.iso | tr | |
dc.rights | info:eu-repo/semantics/openAccess | |
dc.rights | Attribution 4.0 United States | tr_TR |
dc.rights.uri | https://creativecommons.org/licenses/by/4.0/ | |
dc.subject | Eğitim ve Öğretim | tr_TR |
dc.subject | Education and Training | en_US |
dc.subject | Fizik ve Fizik Mühendisliği | tr_TR |
dc.subject | Physics and Physics Engineering | en_US |
dc.title | 2,4 dimethoxybenzylidene-2-hydroxyaniline kristalinin x-ışınları kırınım yöntemi ile yapı çözümü | |
dc.title.alternative | The Structure determination of crystal of 2,4 dimethoxybenzylidene-2-hydroxyaniline by x-ray diffraction method | |
dc.type | masterThesis | |
dc.date.updated | 2018-08-06 | |
dc.contributor.department | Fizik Eğitimi Anabilim Dalı | |
dc.subject.ytm | Diffraction | |
dc.subject.ytm | Crystals | |
dc.subject.ytm | X ray | |
dc.subject.ytm | Crystal structure | |
dc.identifier.yokid | 93645 | |
dc.publisher.institute | Fen Bilimleri Enstitüsü | |
dc.publisher.university | GAZİ ÜNİVERSİTESİ | |
dc.identifier.thesisid | 93645 | |
dc.description.pages | 117 | |
dc.publisher.discipline | Diğer | |