Show simple item record

dc.contributor.advisorKılıç, Adem
dc.contributor.authorYenilmez, Gönül
dc.date.accessioned2021-05-07T12:30:15Z
dc.date.available2021-05-07T12:30:15Z
dc.date.submitted1997
dc.date.issued2018-08-06
dc.identifier.urihttps://acikbilim.yok.gov.tr/handle/20.500.12812/621594
dc.description.abstractÖZET Bu çalışmada 1,4,7, 10, 13-pentaoksasiklopentadekan-2-metanamin bileşiğinin sentezi gerçekleştirildi. Daha sonra hekzaklorosiklotrifosfazatrien (trimer) ile 1,4,7,10,13- pentaoksasiklopentadekan-2-metanamin'in reaksiyonu ve oluşan ürünlerin yapılan incelendi. Trimer ile 1,4,7, 10, 13-pentaoksasiklopentadekan-2-metanamin'in aşın miktarı alınarak THF içinde ve argon atmosferinde reaksiyon gerçekleştirildi. Trimer ile 1,4,7, 10, 13-pentaoksasiklopentadekan-2-metanamin'in reaksiyonunda %45 verimle altı tane 1,4,7, 10, 13-pentaoksasiklopentadekan-2- metanamin'in bağlandığı trimer türevi hazırlandı. Elde edilen bu bileşiklerin yapılan, kütle, ER, *H NMR, 13C NMR spektrumlarından ve elementel analizden elde edilen bilgilerle açıklandı.
dc.description.abstract. 3 ABSTRACT ^ v In this study, firstly 1,4,7, 10, 13-pentaoxacyclopentadecane-2-memanamine was prepared. And than the reaction of hexachlorocyclotriphosphazatriene with 1,4,7,10,13- pentaoxacyclopentadecane-2-methanamine was investigated and obtained products were elucidated structurely. The trimer was reacted with an excess amount of 1,4,7,10,13- pentaoxacyclopentadecane-2-methanamine in THF and in an argon atmosphere. Trimer and l,4,7,10,13-pentaoxacyclopentadecane-2-methanamine in THF gave 45 % yield which hexasubstituted trimer. This product was investigated structurally via IR, XH NMR, 13C NMR, mass spectra and elemental analysis so the results were given in the manner.en_US
dc.languageTurkish
dc.language.isotr
dc.rightsinfo:eu-repo/semantics/openAccess
dc.rightsAttribution 4.0 United Statestr_TR
dc.rights.urihttps://creativecommons.org/licenses/by/4.0/
dc.subjectKimyatr_TR
dc.subjectChemistryen_US
dc.titleHekzaklorosiklotrifosfozatrien ile pentaoksasiklopentadekan-2-metanamin`in reaksiyonu
dc.typemasterThesis
dc.date.updated2018-08-06
dc.contributor.departmentKimya Ana Bilim Dalı
dc.subject.ytmHexachlorocyclotriphosphazatriene
dc.subject.ytmPentaoxacyclopentadecane-2-methanamine
dc.identifier.yokid66011
dc.publisher.instituteMühendislik ve Fen Bilimleri Enstitüsü
dc.publisher.universityGEBZE YÜKSEK TEKNOLOJİ ENSTİTÜSÜ
dc.identifier.thesisid66011
dc.description.pages56
dc.publisher.disciplineDiğer


Files in this item

Thumbnail

This item appears in the following Collection(s)

Show simple item record

info:eu-repo/semantics/openAccess
Except where otherwise noted, this item's license is described as info:eu-repo/semantics/openAccess