2-Hidroksi-1 naftaldehidin primer aminlerle schiff bazlarının sentezi ve bazı geçiş metal komplekslerinin hazırlanması
dc.contributor.advisor | Toy, Mehmet | |
dc.contributor.author | Işiklan, Muhammet | |
dc.date.accessioned | 2020-12-09T10:10:55Z | |
dc.date.available | 2020-12-09T10:10:55Z | |
dc.date.submitted | 1997 | |
dc.date.issued | 2020-12-07 | |
dc.identifier.uri | https://acikbilim.yok.gov.tr/handle/20.500.12812/206325 | |
dc.description.abstract | ÖZET Bu çalışmada, 2-Hidroksi-l-naftaldehitin metanol ortamında aromatik primer aminlerle etkileştirilmesi sonucu N-(2-piridil)-2-hidroksi-l-naftaldimin (C16H12N2O) (1), N-(4-metil-2-pridil)-2-hidroksi-l-naftaldimin (C17Hı3N20) (2) ve N~(6-metil-2-pridil)-2- hidroksi-l-naftaldimin(Ci7Hı5N20) (3) schiff bazları sentezlendi.Bu schiffbazı ligandları ile Zn(II), Co(II) ve Cu(II) kompleksleri hazırlandı.Ligandların ve komplekslerin yapıları FTIR, ^-NMR, element analizi,magnetik süsseptibilite ve X-ışınlan kristallografisi verilerinden faydalanılarak aydınlatıldı. Anahtar Kelimeler: 2-Hidroksi-l-naftaldehit, Schiff bazları, Schiffbazı kompleksleri. | |
dc.description.abstract | Ill ABSTRACT In this study, N-(2-pyridyl)-2-hydroxy-l-naphtaIdimine(l), N-(4-methyl-2- pyridyl)~2-hydroxy- l-naphtaldimine(2) and N-(6-methyl-2-pyridyl)-2-hydroxy- 1 - naphtaldimine (3) schiff bases were synthezided by reaction of 2-hydroxy-l- naphthaldehyde with aromatic primary amines in methanol.Using these schiff base ligands Zn(II), Co(II) and Cu(II) complexes were prepared. The structure of the ligands and their complexes were determined by elemental analyses, magnetic susseptibility, FTIE^H-NMR spectral data and X-ray Crystallograpy. Key words: 2-Hydroxy-l-naphthaldehyde, Schiff bases, Schiff base complexes. | en_US |
dc.language | Turkish | |
dc.language.iso | tr | |
dc.rights | info:eu-repo/semantics/embargoedAccess | |
dc.rights | Attribution 4.0 United States | tr_TR |
dc.rights.uri | https://creativecommons.org/licenses/by/4.0/ | |
dc.subject | Kimya | tr_TR |
dc.subject | Chemistry | en_US |
dc.title | 2-Hidroksi-1 naftaldehidin primer aminlerle schiff bazlarının sentezi ve bazı geçiş metal komplekslerinin hazırlanması | |
dc.title.alternative | Synthesis of schiff bases by 2-hydroxy-1 naphthaldehyde and primary amines and preparation of their some transitions metal complexes | |
dc.type | masterThesis | |
dc.date.updated | 2020-12-07 | |
dc.contributor.department | Kimya Anabilim Dalı | |
dc.subject.ytm | Transition metals | |
dc.subject.ytm | Metal complexes | |
dc.subject.ytm | Amines | |
dc.subject.ytm | Schiff bases | |
dc.identifier.yokid | 67039 | |
dc.publisher.institute | Fen Bilimleri Enstitüsü | |
dc.publisher.university | KIRIKKALE ÜNİVERSİTESİ | |
dc.identifier.thesisid | 67039 | |
dc.description.pages | 74 | |
dc.publisher.discipline | Diğer |