Mikrodalga yöntemiyle çözücüsüz ortamda amit sentezi
| dc.contributor.advisor | Gümgüm, Bahattin | |
| dc.contributor.author | Meriç, Nermin | |
| dc.date.accessioned | 2020-12-07T08:36:35Z | |
| dc.date.available | 2020-12-07T08:36:35Z | |
| dc.date.submitted | 2006 | |
| dc.date.issued | 2018-08-06 | |
| dc.identifier.uri | https://acikbilim.yok.gov.tr/handle/20.500.12812/115890 | |
| dc.description.abstract | Bu çalısmada, mikrodalga yöntemiyle çözücüsüz ortamda -hidroksiizobütirik asit ileanilin türevleri etkilestirilerek bes yeni amit elde edildi. Sonra farklı güçler farklı sürelerdeuygulanarak bu amitleri en yüksek verimle elde etmek için gereken en uygun kosullararastırıldı. Sentezlenen amitler IR, NMR, UV-görünür alan ve X ısınları spektroskopileriile karakterize edildi. Ayrıca DL-mandelik asit ile anilin türevleri ve 2-pikolilaminetkilestirilerek yedi tane daha amit elde edildi. | |
| dc.description.abstract | In this study, five new amide compounds were synthesized by the reaction of -hydroxybutiric acid with aniline derivatives by microwave irradiation in solvent freemedium. In order to improve yield, optimum conditions were investigated by exertingdifferent powers at different irradiation times. The amides were characterized by IR,NMR, UV-vis and X-ray spectroscopies. Furthermore, seven additional amides wereobtained from the reaction of DL-mandelic acid and aniline derivatives and 2-picolylamine. | en_US |
| dc.language | Turkish | |
| dc.language.iso | tr | |
| dc.rights | info:eu-repo/semantics/openAccess | |
| dc.rights | Attribution 4.0 United States | tr_TR |
| dc.rights.uri | https://creativecommons.org/licenses/by/4.0/ | |
| dc.subject | Kimya | tr_TR |
| dc.subject | Chemistry | en_US |
| dc.title | Mikrodalga yöntemiyle çözücüsüz ortamda amit sentezi | |
| dc.title.alternative | Solvent-free preparation of amides under microwave irridiation | |
| dc.type | masterThesis | |
| dc.date.updated | 2018-08-06 | |
| dc.contributor.department | Kimya Anabilim Dalı | |
| dc.identifier.yokid | 368939 | |
| dc.publisher.institute | Fen Bilimleri Enstitüsü | |
| dc.publisher.university | DİCLE ÜNİVERSİTESİ | |
| dc.identifier.thesisid | 255027 | |
| dc.description.pages | 73 | |
| dc.publisher.discipline | Diğer |
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